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Sodium trichloroacetate

From Crystal growing


   Sodium trichloroacetate   
Names: sodium trichloroacetate
Formula: CCl3COONa
Molar mass: 185.369 g/mol
Density: 1.5 g/cm3
Crystal system: monoclinic
α=90°, γ=90°
Shapes:
https://en.crystalls.info/w/uploads/media/c/c4/Tetragonal_pedion.json

Color: colorless
Melting point: 200 °C473.15 K <br />392 °F <br />851.67 °R <br />
Stability: rapidly erodes
Hardness: fragile
Toxicity: non-toxic
LD50=6000mg/kg

Description

Organic compound, salt of alkaline metal sodium and organic trichloroacetic acid. Doesn't form water hydrates.

Chemical equation:

CCl3COOH + NaHCO3 = CCl3COONa + H2O + CO2
2CCl3COOH + Na2CO3 = 2CCl3COONa + H2O + CO2
CCl3COOH + NaOH = CCl3COONa + H2O


For preparation of 100.00g of sodium trichloroacetate а 45.32g of sodium hydrocarbonate or 28.59g of sodium carbonate or 21.58g of sodium hydroxide is required.

Add acid to the flask, then add small parts of sodium compound with stirring until heating will stop (attention, the solution may boil!) or, if you use carbonate, until carbon dioxide emission will stop.

Notes

It's probable that there is an unknown hydrate which forms from water solution, because crystals erode in the open air within minutes. But there is no information about it in the literature.

For crystal storing use hermetic vessel with wadding moistened with such solution near the crystal. You can use such alternatives as vessel with vaseline or vegetable oil, organic non-hygroscopic solvent (kerosene or liquid paraffin). Also you can use acrylate polymer or another kinds of solidifying plastic.

Temperatureg/100,00 g waterg/100,00 g acetone
25°C298.15 K <br />77 °F <br />536.67 °R <br />557.3
Soluble in ethanol and methanol. Insoluble in diethyl ether.



Sources